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Download Analytical Chemistry of Zirconium and Hafnium by Anil K. Mukherji, R. Belcher and M. Frieser (Auth.) PDF

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By Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)

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19, 89 (1937). OSTROUMOV, E. , Zavod. Lab. 6, 16 (1937). WELCHER, F . , Organic Analytical Reagents, Van Nostrand, New York, 1947, Vol. 1, p. 323. 28. ALLEN, E. , / . Amer. Chem. Soc. 25, 421 (1903). 29. , Z . Anal. Chem. 78, 133 (1929); 86, 13 (1931). 30. RAY, P. and CHATTOPADHYA, A. , Z . Anorg. Chem. 169, 199 (1926). 31. HOLNESS, H . and KEAR, R. , Analyst, 74, 597 (1949). 32. PURUSHOTTAM, A. and RAGHAVA R A O , B. S. , Analyst, 75, 555 (1950). 33. PURUSHOTTAM, A. and RAGHAVA RAO, B. S. , Rec.

ALIMARIN, I. P. and HAN-HSI HEN, Zhur. Anal. Khim. 16, 162 (1961). 81. OKA, Y. , Japan Analyst, 13, 207 (1964). 82. , and TATLOW, J. , Anal. Chim. Acta, 10, 34 (1954). 83. GAVIOLI, G. , Met. Ital. 42, 179 (1950). 84. HAHN, R. , Anal. Chem. 21, 1579 (1949). 85. HAHN, R. B. and BAGINSKI, E. , Anal. Chim. Acta, 14, 45 (1956). 86. HAHN, R. B. , / . Amer. Chem. Soc. 77,4777 (1955); Anal. Chem. 28, 414 (1956). 87. HILL, J. H. and MILES, M. , Anal. Chem. 31, 252 (1959). 88. KUMINS, C. , Anal. Chem. 19, 376 (1947).

No interferences (82-89, 133-137) Less sol. than Zr mandelate (82,90-97) No advantage over mandelic acid (98, 94-97) 2 o ö in 5 > H o-, m- and /7-Fluoromandelic Zr(FC8H603)4 acid Zr0 2 No advantage over mandelic acid (82, 99) Zr(F3C8H403)4 ZrOo No advantage over mandelic acid (82) Trifluoromandelic acid > < 3 2 o TABLE 2—cont. 6 N H 2 S0 4 . F does not interfere (13, 1, 21, 106, 108, 109, 110) Neocupferron Zr(NeOCuP)4 ZrOa Less sol. than cupferron (108) ZrOa or the precipitate > > r < H O > o SB m Ά O o § S > z σ Si g 8-Hydroxyquinoline ZrO(C9H609)2 at 20°C; >60°C, pptedas Zr [Zr(C9H6NO)4] Zr02 Ppted from dil HN0 3 in presence of NH4OAc.

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